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The half-life of CuHSA demetallation in the presence of EDTA was 2030 min (Fig

Ran, C.S

Primary endpoint: change in body weight

Taken together, these pooled safety analyses (119123) and CV outcome safety trials (124127), together with review of published data from numerous clinical trials (39), provide reassuring evidence that the catalytic activity of the DPP-4 molecule can be modulated to enhance the beneficial metabolic effects of its substrates (such as the incretin hormones) without adversely affecting any of the protease-independent metabolic effects discussed above, or interfering with any of its other (non-metabolic) functions

The 10 gm of the sample was put in the mortar with an equal quantity of KBr pallet to make a tablet and the tablet was placed on an instrument holder for the FT-IR analysis